401900 Separation of a disilane and a silacylobutene

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Separation of a disilane and a silacylobutene

Summary

Type: TLC
Application #: 401900
Catalog#: 1634126 - Silica G TLC Plates, w/UV254, aluminum backed, 200um, 20x20cm 25/pk
Detection: UV, 254 nm
Conditions: Eluent: hexane / NEt3 (97.5:2.5)
Authors: Belzner J
Source: Chem Eur J 4 (1998) 852-863


Details


Legend: Rf-values: 1.) 1-[2-(Dimethylaminomethyl)phenyl-2,4,6-tris(isopropyl)phenyl]silyl-2,3-[4,6-bis( isopropyl)-benzo]-4-dimethyl-1-silacyclobutene 0.35 2.) 1,2-Bis[2-(dimethylaminomethyl)phenyl]-1,2-