305230 Heterocyclic Aromatic Amines in Heated Meat

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Heterocyclic Aromatic Amines in Heated Meat

Summary

Type: SPE
Application #: 305230
Catalog#: 730377 - SPE Cartridges, Chromabond, PS-H+, 6ml, PP, 500mg 30/pk
Detection:
Conditions: CHROMABOND® XTR Sample aspiration: The alkaline solution was poured into XTR column. Elution: It was eluted with 50 ml ethyl acetate. CHROMABOND® PS-H+ Sample aspiration: The eluate was passed into PS-H+ column. Washing: The column was washed with 2 ml 0.1 M HCl and 2 ml MeOH. Elution: Compounds were eluted with 2 ml methanol/conc. ammonia (19:1, v/v) Evaporation: Sample was evaporated to dryness (nitrogen). Reconstitution: Extract was dissolved in 100 mg methanol.
Authors: Damasius, J.; Venskutonis, P.R.
Source: FOODBALT 2008, 117-120