305080 Extraction of veterinary drugs in fish with an ASPEC system

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Extraction of veterinary drugs in fish with an ASPEC system

Summary

Type: SPE
Application #: 305080
Detection:
Conditions: Automated SPE method on Gilson GX-271 ASPEC system: Column conditioning: 2 x 3 ml n-hexane, drying by vacuum, then 3 ml 0.5 % acetic acid in ethyl acetate; Do not let run the column dry! Sample aspiration: 5 - 8 ml/min, then 10 - 12 min drying Washing: 10 ml methanol Elution: 5 ml 10 % triethanolamine in methanol
Authors: Stevens, J.M.; Crawford, M.; Halvorson, M.; Ubben, S.
Source: GIT Spezial, Separation 1/2009, 16-17