304620 Extraction of tetracyclines and sulfadiazine from percolation water

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Extraction of tetracyclines and sulfadiazine from percolation water

Summary

Type: SPE
Application #: 304620
Catalog#: 732108 - SPE Cartridges, Chromabond LV, HR-P, 15ml, 200mg, 30/pk
Detection:
Conditions: Column conditioning: 2 mL methanol, then 2 mL dest. water (Do not let run the column dry.) Sample aspiration: The prepared sample is passed through the column by vacuum (flow rate 4 mL/min) Washing: 2 x 2 mL dest. water Drying: air Elution (tetracyclines): 2 x 1 mL 0.5 % trichloroacetic acid in methanol Elution (sulfadiazine): 2 x 1 mL methanol
Authors: Engels, H.
Source: Diss., ISBN 3-86537-376-3, Göttingen, Germany 2004