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16 EPA-PAHs from Soil with CHROMABOND
Summary
Type: SPEApplication #: 302820
Catalog#: 730755 - SPE Cartridges, Chromabond, Easy, 6ml, PP, 200mg 30/pk
Detection: HPLC: with Nucleosil 100-5 C18 PAH GC: Optima 5 MS, 30m, 0,25 mm ID, 0,25µm FD
Conditions: Sample: soil or sludge
Conditioning: 3 ml MeOH, 3 ml Water
Application: 250 ml sample solution
Washing: 2 x 3 ml Water - MeOH (95:5, v/v)
Drying: Vacuum
Elution: 2 x 1 ml Dichlormethane (for GC-Analytik)
or for HPLC-Analytic: Concentrate dichlormethane in a nitrogen atmosphere and dissolve in acetonitrile
Authors: Macherey-Nagel
Source: LC Department
Details
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