302190 A Method for the Determination of 7 Anti-arrhythmic Drugs and their Metabolites in Serum
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A Method for the Determination of 7 Anti-arrhythmic Drugs and their Metabolites in Serum
Summary
Type: SPEApplication #: 302190
Catalog#: 730002 - SPE Cartridges, Chromabond, C18, 3ml, PP, 200mg, 50/pk
Detection: Portions of serum (20µl) were analysed by HPLC on a EC 250/4 NUCLEOSIL® 100-5 C18 (Cat. No. 720014.40) according to Application No. 120790
Conditions: Conditioning: 3 ml methanol, then 3 ml water Sample application: Slowly force or aspirate 1 ml serum through the column. Washing: 2 ml water, then 1 ml acetonitrile Elution: with methanol con
Authors: Brandsteterová E Ferencová A
Source: Katedra analytickej chemie Slovenská techniká univerzita Radlinskeho 9 81237 Bratislava Slovebská republika Doslo dna 13III1998
Details
Legend: Extraction recoveries of 0,06 - 0,43µg/ml of added drugs to serum were in the range 81,4 - 90,7%.