213100 Silylation with BSA in combination with other silylation reagents

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Silylation with BSA in combination with other silylation reagents

Summary

Type: GC
Application #: 213100
Detection: GC
Conditions: a) BSA alone silylates all sterically unhindered hydroxyl groups of the steroid skeleton.
b) Addition of TMCS will enable reaction of moderately hindered OH groups.
c) After addition of TSIM even strongly hindered hydroxyl groups will react.
Authors: Macherey-Nagel
Source: GC department (2007)


Details


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