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Separation of phenols (EPA 528)
Summary
Type: GCApplication #: 212840
Catalog#: 725820.30 - GC Column, Optima-5 MS-A, 0.25mm, 0.25um, 30m
Detection: GC/MS, 280 °C, scan range: 35 - 550 amu
Conditions: Injection volume: 1 ul, pulsed splitless (for 0.5 min), pulsed pressure 50 psi for 0.5 min
Injection temperature: 220 °C
Carrier gas: Helium, 1.3 ml/min
Temperature: 40 °C for 1 min --> 200 °C, 12 °C/min --> 300 °C, 30 °C/min for 1 min
Authors: GC department
Source: Macherey-Nagel
Details
Legend: 1. phenol 2. 2-chlorophenol-3,4,5,6-d4 3. 2-chlorophenol 4. 2-methylphenol 5. 2-nitrophenol 6. 2,4-dimethylphenol-3,5,6-d3 7. 2,4-dimethylphenol 8. 2,4-dichlorophenol 9. 4-chloro-3-methylphen