202230 Separation of 2-tert.-Butyl-5-bromomethylene 1,3-dioxane enantiomers

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Separation of 2-tert.-Butyl-5-bromomethylene 1,3-dioxane enantiomers

Summary

Type: GC
Application #: 202230
Catalog#: 723360.50 - GC Column, FS LIPODEX A, 0.25 mm, 50 m
Detection: FID 250 °C, 2^7
Conditions: Injection volume: 0.5 ul (2% in methylene chloride)
Carrier gas: 130 kPa H2 (2.0 ml/min)
Split: 92 ml/min
Temperature: 105 °C
Authors: Macherey-Nagel
Source: GC department


Details


Legend: 2-tert.-Butyl-5-bromomethylene 1,3-dioxane