110190 Analysis of oxcarbazepine (antikonvulsivum) from serum

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Analysis of oxcarbazepine (antikonvulsivum) from serum

Summary

Type: HPLC
Application #: 110190
Detection: UV, 200nm
Conditions: Eluents:
A) 2 mmol NaH2PO4, 1 g 1-hexanesulfonic acid adjusted with H3PO4 to pH 2,5
B) Acetonitril

Gradient: A/B 82:18, in 25 min. to 59:41, then for 5 min. 10:90

Flow rate: 0,8 mL/min.
Inj. vol.: 25 ul
Temperature: 40 °C
Authors: Kothe
Source: Laboratory Dr Krone Prof Hagedorn Herford Germany