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Semisynthesis of 14C-labelled leupeptin
Summary
Type: HPLCApplication #: 107820
Detection: UV, 205nm
Conditions: eluent: 1% H3PO4 - CH3CN (83:17, v/v)
flow rate 1.5ml/min
Authors: Saino T
Source: Chem Pharm Bull 30 (1982) 2319 - 2325
Details
Legend: Fig. 2. HPLC of authentic Ac-D-Leu-L-Leu-L-Argal (A) and Ac-[U-14C]-Leu-L-Leu-L-Argal (B) synthesized from Ac-L-[U-14C]-Leu-OH and H-L-Leu-L-Argal (OBu)2 using diphenylphosphoryl azide as a condensi