105960 Identification of the ( )- and (-)-enantiomers of chiral chlordane compounds using chiral HPLC

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Identification of the ( )- and (-)-enantiomers of chiral chlordane compounds using chiral HPLC

Summary

Type: HPLC
Application #: 105960
Catalog#: 720125.40 - MN HPLC Column, Nucleodex B-PM, 100A, 5um, 4x200mm
Detection: RI
Conditions: sample: 5 - 20 μl of 0.1 - 0.5 % solutions in MeOH
eluent: 80 % MeOH / 20 % 0.1 % aqueous TEAA (pH 4.0)
flow rate: 0.7 ml/min
Authors: Müller MD
Source: Anal Chem 1994 66 2155 - 2162


Details


Legend: Fig. 1: HPLC chromatograms of racemic chlordane compounds using (a - d) RI detection (sensitivity 2 x 10 -5 RI units) and (e - h) chiroptical detection (sensitivity ± 40 mV) using polychromatic ligh