105620 Separation of the four optical isomers of a dihydropyridine calcium channel antagonist

Contact an Account Manager

Separation of the four optical isomers of a dihydropyridine calcium channel antagonist

Summary

Type: HPLC
Application #: 105620
Catalog#: 720099.46 - MN HPLC Column, Nucleosil, 100A, 5um, 4.6x250mm
Detection: UV, 229nm
Conditions: eluent: 0.1% acetonitrile and 4% 2-propanol in isooctane (2,2,4-trimethylpentane)
flow rate 2.0ml/min
temperature 50°C
Authors: Ward, K.D. et al.
Source: J. Chromatogr. 478 (1989) 169–179


Details


Legend: Fig. 1. HPLC separation of the RS-93522-004 bis-camphanate diastereomers, sample concentration approx. 0.3mg/ml, sample loading approx. 6µg.