104440 Highly sensitive differential pulse amperometric detection of second generation antitumour platinum compounds in HPLC effluents

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Highly sensitive differential pulse amperometric detection of second generation antitumour platinum compounds in HPLC effluents

Summary

Type: HPLC
Application #: 104440
Detection: polarographic detection: PAR 310 in DPP mode, 100mV pulse, medium drop size, 0.5sec pulse interval
Conditions: eluent: 10% methanol in aqueous 0.1M NaNO3
flow rate 1ml/min
Authors: van der Vijgh W.J.F. et al.
Source: Chromatographia 17 (1983) 333–336


Details


Legend: Fig. 6. Chromatograms at I. 6min, II. 13min; III. 21min and IV. 28min after mixing of equal volumes of TNO-6 (105.5µg/ml water) and 0.30M NaCl, peaks: A. oxygen, B. TNO-1, C. TNO-6.