100250 Silver complexation LC for fast high resolution separations of triacylglycerols

Contact an Account Manager

Silver complexation LC for fast high resolution separations of triacylglycerols

Summary

Type: HPLC
Application #: 100250
Detection: FID
Conditions: eluent A: toluene - hexane (1:1, v/v),
eluent B: toluene - ethyl acetate (9:1, v/v),
eluent C: toluene - 98% formic acid (500ml:40μl),
gradient program: A:B:C at 0min (injection) 94:6:0, at 2.5min 92:8:0, at 7min 75:25:0, at 10min 10:90:0, at 10.1 to 15min 0:0:100 (column regeneration), at 15.1 to 18min 94:6:0, at 18min next injection,
flow rate: 1.5ml/min.
Authors: Jeffrey B S J
Source: J Am Oil Chem Soc 68 (1991) 289 - 293


Details


Legend: Comparative isometric plot of silver complexation separations of TAG from cocoa butter and Coberine (a cocoa butter equivalent).